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Effect of different high viscosity modifiers on rheological properties of high viscosity asphalt

《结构与土木工程前沿（英文）》 2021年 第15卷 第6期   页码 1390-1399 doi: 10.1007/s11709-021-0775-z

摘要： High viscosity asphalt (HVA) has been a great success as a drainage pavement material. However, the larger porosity of drainage asphalt mixtures weakens the cohesion and adhesion and leads to premature rutting, water damage, spalling and cracking. The purpose of this study was to investigate the rheological properties of HVA prepared using different high viscosity modifiers through conventional tests, Brookfield viscosity tests, dynamic shear rheometer tests and bending beam rheometer tests. The conventional performance results demonstrated SBS + rubber asphalt (SRA-1/2) exhibited excellent elastic recovery and low-temperature flexibility. The 60°C dynamic viscosity results indicated TPS + rubber asphalt (TRA) had the excellent adhesion. The rotational viscosity results and rheological results indicated that SRA-2 not only exhibited excellent temperature stability and workability, as well as excellent resistance to deformation and rutting resistance, but also exhibited excellent low-temperature cracking resistance and relaxation performance. Based on rheological results, the PG classification of HVA was 16% rubber + asphalt for PG76-22, 20% rubber + asphalt for PG88-22, TRA and SRA-1/2 for PG88-28. From comprehensive evaluation of the viscosity, temperature stability and sensitivity, as well as high/low temperature performance of HVA, SRA-2 was found to be more suited to the requirements of drainage asphalt pavement materials.

关键词： high viscosity asphalt     rheological properties     rubber     modifier     viscosity    

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新型高黏度改性沥青的研发和应用

杨林江

《中国工程科学》 2008年 第10卷 第12期   页码 92-96

摘要：

针对杭州湾大桥桥面铺装对高黏度改性沥青的技术要求，研发了一种新型高黏度改性沥青［1］。通过分析基质沥青、SBS、化学助剂的红外光谱，在研究沥青改性过程中微观结构变化规律的基础上，提出了采用SBS加化学接枝反应剂（增黏剂）TW-1和增容剂TW-2的沥青改性配伍设计，使改性沥青在提高低温延度、弹性恢复能力的同时，大幅度提升了60 ℃动力黏度，而施工和易性不受影响，产品在杭州湾大桥工程中得到了成功的应用。

关键词： 杭州湾大桥     高黏度改性沥青     配伍机理     红外光谱分析     路用性能     施工性能    

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Linear viscoelastic behavior of asphalt binders and mixtures containing very high percentages of reclaimedasphalt pavement

《结构与土木工程前沿（英文）》   页码 1211-1227 doi: 10.1007/s11709-023-0983-9

摘要： The primary aim of this study is to correlate the impact of aggregates, if any, on the viscoelastic behavior of rejuvenated asphalt mixtures containing very high amounts of reclaimed asphalt pavement (RAP) (> 50%). First, gradation of 100% RAP was rectified, using a modified Bailey method by adding virgin aggregates to achieve two coarse dense-graded and one fine dense-graded blends. Complex modulus test was then performed from −35 to +35 °C and 0.01–10 Hz. In addition to performance grade (PG) testing, extracted and recovered binders from different asphalt mixtures underwent shear complex modulus test within −8 °C to high temperature PG and frequencies from 0.001 to 30 Hz. Cole−Cole, Black space, complex modulus and phase angle master curves were constructed and Shift-Homothety-Shift in time-Shift (SHStS) transformation was used to compare the linear viscoelastic behavior of asphalt binders and mixtures. The influence of aggregates on the viscoelastic behavior of asphalt mixtures depends on temperature and/or frequency. The role of asphalt binders in the behavior of asphalt mixtures is more pronounced at high temperatures and the effect of the aggregate structure increases as the temperature falls. The maximum difference (60% to 70%) in the viscoelastic behavior of the binder and mixture based on SHStS transformed Cole−Cole curves is within the phase angle of 15°–20°.

关键词： RAP     complex modulus     SHStS transformation     rejuvenation     behavior of asphalt binder and mixture    

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Development and road performance of clear asphalt with high transparency and adhesion

《结构与土木工程前沿（英文）》 2023年 第17卷 第2期   页码 238-255 doi: 10.1007/s11709-022-0898-x

摘要： Clear asphalt (CA) currently used in light-colored asphalt mixtures (LCAM) exhibits poor transparency and adhesion. Therefore, a highly transparent CA (HCA) modified using a silane coupling agent (KH550) was prepared. Furthermore, LCAM was prepared by mixing CA and limestone aggregates. The properties of the HCA and ordinary CA (OCA) were characterized using conventional asphalt tests, optical tests, pull-off tests, ultraviolet aging tests, dynamic shear rheometry, Fourier-transform infrared spectroscopy, differential scanning calorimetry, and scanning electron microscopy. Whereas Marshall, moisture resistance, wheel tracking, trabecular bending, and British pendulum tests were employed for the LCAM. The transmittance and spectral reflectance of the HCA were 123.30 and 3.74 times greater than those of the OCA, respectively. The complex modulus and viscosity-aging index of the HCA were 48% and 53% less than those of the OCA, respectively. After modification with KH550, the Marshall stability ratio, tensile strength ratio, and flexural strain of the HCA-prepared LCAM increased by 12.92%, 25.06%, and 23.90%, respectively. However, the rutting resistance of the HCA-prepared LCAM was 14.3% less than that of the OCA-prepared LCAM. The comprehensive performances of the HCA and HCA-prepared LCAM were 49.2% and 10.3% greater than those of the OCA and OCA-prepared LCAM, respectively, indicating a high application value in the future.

关键词： light-colored asphalt pavement     orthogonal test     road performance     spectral reflectance     silane-coupling agent    

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saccharification and fermentation of sweet potato powder for the production of ethanol under conditions of very high

Yinxiu CAO, Hongchi TIAN, Kun YAO, Yingjin YUAN

《化学科学与工程前沿（英文）》 2011年 第5卷 第3期   页码 318-324 doi: 10.1007/s11705-010-1026-3

摘要： Due to its merits of drought tolerance and high yield, sweet potatoes are widely considered as a potential alterative feedstock for bioethanol production. Very high gravity (VHG) technology is an effective strategy for improving the efficiency of ethanol fermentation from starch materials. However, this technology has rarely been applied to sweet potatoes because of the high viscosity of their liquid mash. To overcome this problem, cellulase was added to reduce the high viscosity, and the optimal dosage and treatment time were 8 U/g (sweet potato powder) and 1 h, respectively. After pretreatment by cellulase, the viscosity of the VHG sweet potato mash (containing 284.2 g/L of carbohydrates) was reduced by 81%. After liquefaction and simultaneous saccharification and fermentation (SSF), the final ethanol concentration reached 15.5% (v/v), and the total sugar conversion and ethanol yields were 96.5% and 87.8%, respectively.

关键词： bioethanol     sweet potato     very high gravity     viscosity reduction     simultaneous saccharification and fermentation    

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Effect of carbon black on the dynamic moduli of asphalt mixtures and its master curves

Chuangmin LI, Fanbo NING, Yuanyuan LI

《结构与土木工程前沿（英文）》 2019年 第13卷 第4期   页码 918-925 doi: 10.1007/s11709-019-0526-6

摘要： Modulus is one of the main parameters during the design of asphalt pavement structure, the newest specifications of China gives the dynamic moduli ranges of commonly used asphalt mixtures with base asphalt (BA) or styrene-butadiene-styrene modified asphalt (SBS MA), while the moduli ranges of mixtures with carbon black modified asphalt (CB MA) are not recommended. To investigate the CB effect on the dynamic moduli of CB MA mixtures, one commonly used asphalt mixture (AC-20) was designed with BA, SBS MA, and CB MA, respectively. Then, the uniaxial compression dynamic modulus tests were conducted at different temperatures and loading frequencies, the master curves of asphalt mixtures were analyzed based on the time-temperature equivalence principle. The results show that ith increasing loading frequency, the temperature dependence of dynamic moduli of all asphalt mixtures tend to be less obvious. Both SBS and CB can decrease the temperature sensitivity of asphalt mixture, the SBS MA mixture has the lowest temperature sensitivity, followed by CB MA and BA mixture. In addition, CB and SBS can obviously improve the dynamic modulus of the BA mixture, enhance the anti-deformation performance of pavement structure, and the improvement effect of CB is almost the same with SBS.

关键词： dynamic modulus     carbon black     master curve     modified asphalt     asphalt mixture    

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New approach to determine the plastic viscosity of self-compacting concrete

M. BENAICHA,X. ROGUIEZ,O. JALBAUD,Y. BURTSCHELL,A. Hafidi ALAOUI

《结构与土木工程前沿（英文）》 2016年 第10卷 第2期   页码 198-208 doi: 10.1007/s11709-015-0327-5

摘要： The rheology of concrete is best measured with the use of a rheometer. The slump flow test gives a good indication of the flowability of the mixture and is therefore still used extensively to judge the workability of SCC mixtures. However, this test presents some defects. The objective of this paper is to develop a new methodology for measuring the workability of a SCC. In this article, we have proposed a correlation between the plastic viscosity of concrete, the time and the characteristics of the flow final profile from the V-funnel coupled to a Plexiglas horizontal channel. The proposed approach, verified by experimental results, represents a simple, economical and usable tool on building site, and it allows to characterize rheologically the SCC from its flow. The comparison between our approach and the experimental values of the plastic viscosity shows that, in a laboratory or on site, instead of using a rheometer we can use our approach to characterize the rheological behavior of a SCC.

关键词： rheology     viscosity     V-funnel     flow profile     rheometer     behavior    

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Outdoor aging of road asphalt and SBS modified asphalt

Li XIANG, Juan TU, Jian CHENG, Guohe QUE

《化学科学与工程前沿（英文）》 2011年 第5卷 第1期   页码 35-42 doi: 10.1007/s11705-010-0551-4

摘要： The process of performance degradation of road asphalt (RA) is regarded as aging. At present, better understanding of the thermal-oxidative aging of asphalt is achieved and the corresponding method to evaluate this process is developed; meanwhile, photo-oxidative aging (aging in an atmospheric environment, which is referred to as “outdoor aging” in this paper) of asphalt remains at the initial stages of scientific exploration. The outdoor natural ultraviolet (UV) aging of RA and SBS modified asphalt (SBSMA) are investigated in this study. The experimental results show that the basic performances of RA and SBSMA present similar change tendencies. The softening point increased, while the penetration and ductility decreased as the outdoor aging time passed by, and the 5°C ductility (ductility measured at 5°C) of SBSMA decreased very quickly. The group components of RA and SBSMA also change during UV aging. The content of asphaltene rose and that of aromatics and saturates decreased, while the content of resins changed insignificantly. Moreover, the Fourier transform infrared (FTIR) graphs show that the content of sulfoxide and carbonyl groups in RA and SBSMA increased significantly during the outdoor aging process.

关键词： asphalt     SBS     modified road asphalt     outdoor aging     ultraviolet    

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Fatigue of asphalt binder, mastic and mixture at low temperature

Dong WANG, Linbing WANG, Guoqing ZHOU

《结构与土木工程前沿（英文）》 2012年 第6卷 第2期   页码 166-175 doi: 10.1007/s11709-012-0157-7

摘要： The fatigue damage is one of the most common distresses observed on the asphalt concrete pavement. To thoroughly understand the fatigue of asphalt concrete, the behaviors of the major components of asphalt concrete under cyclic loading are investigated respectively in this study. A new experiment method is developed to evaluate the performances of asphalt binder, mastic and fine aggregates mixture under cyclic tensile loading. The fatigue test results of asphalt binder show that the fatigue performance of asphalt binder is closely related with loading magnitude, temperature and loading rate. Mastic specimens with different filler content are tested and the results indicate that mastic specimens with 30% filler content show better fatigue resistance and higher permanent strain. The micro-structure analysis of mastic and mixture indicates that the fatigue resistance is closely related with the air void content of specimen. 3D digital specimens are developed to model the fatigue of the asphalt binder, mastic and mixture specimens based on the finite element method (FEM). Fatigue damage of asphalt concrete is simplified by a damage model. With proper selection of damage parameters, the simulation results agree well with laboratory test results and can be used as a basis for future fatigue research.

关键词： fatigue     asphalt mixture     asphalt binder     mastic     finite element method (FEM)     X-ray tomography    

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Effect of styrene-butadiene-styrene copolymer on the aging resistance of asphalt: An atomistic understanding

《结构与土木工程前沿（英文）》 2021年 第15卷 第5期   页码 1261-1276 doi: 10.1007/s11709-021-0761-5

摘要： To reveal the potential influence of styrene-butadiene-styrene (SBS) polymer modification on the anti-aging performance of asphalt, and its mechanism, we explored the aging characteristics of base asphalt and SBS-modified asphalt by reaction force field (ReaxFF) and classical molecular dynamics simulations. The results illustrate that the SBS asphalt is more susceptible to oxidative aging than the base asphalt under oxygen-deficient conditions due to the presence of unsaturated C=C bonds in the SBS polymer. In the case of sufficient oxygen, the SBS polymer inhibits the oxidation of asphalt by restraining the diffusion of asphalt molecules. Compared with the base asphalt, the SBS asphalt exhibits a higher degree of oxidation at the early stage of pavement service and a lower degree of oxidation in the long run. In addition, SBS polymer degrades into small blocks during aging, thus counteracting the hardening of aged asphalt and partially restoring its low-temperature cracking resistance.

关键词： SBS asphalt     oxidative aging     asphalt hardening     ReaxFF     molecular dynamics    

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Hierarchical approach for fatigue cracking performance evaluation in asphalt pavements

Ibrahim ONIFADE, Yared DINEGDAE, Björn BIRGISSON

《结构与土木工程前沿（英文）》 2017年 第11卷 第3期   页码 257-269 doi: 10.1007/s11709-017-0410-1

摘要： In this paper, a hierarchical approach is proposed for the evaluation of fatigue cracking in asphalt concrete pavements considering three different levels of complexities in the representation of the material behaviour, design parameters characterization and the determination of the pavement response as well as damage computation. Based on the developed hierarchical approach, three damage computation levels are identified and proposed. The levels of fatigue damage analysis provides pavement engineers a variety of tools that can be used for pavement analysis depending on the availability of data, required level of prediction accuracy and computational power at their disposal. The hierarchical approach also provides a systematic approach for the understanding of the fundamental mechanisms of pavement deterioration, the elimination of the empiricism associated with pavement design today and the transition towards the use of sound principles of mechanics in pavement analysis and design.

关键词： fatigue cracking     energy based     crack initiation     mechanistic approach     pavement analysis    

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A dimensional analysis on asphalt binder fracture and fatigue cracking

Qian ZHAO, Zhoujing YE

《结构与土木工程前沿（英文）》 2018年 第12卷 第2期   页码 201-206 doi: 10.1007/s11709-017-0402-1

摘要： Fracture and fatigue cracking in asphalt binder are two of most serious problems for pavement engineers. In this paper, we present a new comprehensive approach, which consists both of dimensional analysis using Buckingham Theorem and -integral analysis based on classic fracture mechanics, to evaluate the fracture and fatigue on asphalt binder. It is discovered that the dimensional analysis could provide a new perspective to analyze the asphalt fracture and fatigue cracking mechanism.

关键词： Dimensional analysis     asphalt     fracture     fatigue cracking    

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The investigation of fly ash based asphalt binders using atomic force microscope

Rajan SAHA, Kyle MALLOY, Emil BAUTISTA, Konstantin SOBOLEV

《结构与土木工程前沿（英文）》 2017年 第11卷 第4期   页码 380-387 doi: 10.1007/s11709-017-0437-3

摘要： Atomic Force Microscope (AFM) is a relatively new technique for investigation of construction materials. In this study AFM was used to investigate the interaction of asphalt binder with fly ash. Fly ash is a coal combustion byproduct of electric power utilities having pozzolanic properties and commonly used in Portland cement concrete. In this study, an investigation was made by using different types of fly ash with two types of asphalt binders such as PG 58-28 and PG 64-28. Asphalt microstructure is divided into four subgroups such as Saturates, Aromatics, Resins and Asphaltenes (SARA). These four phases can be distinguished by the atomic force microscope. The interaction of these phases affected by introducing fly-ash was investigated and correlation with rheological properties was observed.

关键词： AFM     fly ash     bee     rheology     asphalt    

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A critical review of ash slagging mechanisms and viscosity measurement for low-rank coal and bio-slags

Md Tanvir ALAM, Baiqian DAI, Xiaojiang WU, Andrew HOADLEY, Lian ZHANG

《能源前沿（英文）》 2021年 第15卷 第1期   页码 46-67 doi: 10.1007/s11708-020-0807-8

摘要： Gasification or combustion of coal and biomass is the most important form of power generation today. However, the use of coal/biomass at high temperatures has an inherent problem related to the ash generated. The formation of ash leads to a problematic phenomenon called slagging. Slagging is the accumulation of molten ash on the walls of the furnace, gasifier, or boiler and is detrimental as it reduces the heat transfer rate, and the combustion/gasification rate of unburnt carbon, causes mechanical failure, high-temperature corrosion and on occasions, superheater explosions. To improve the gasifier/combustor facility, it is very important to understand the key ash properties, slag characteristics, viscosity and critical viscosity temperature. This paper reviews the content, compositions, and melting characteristics of ashes in differently ranked coal and biomass, and discusses the formation mechanism, characteristics, and structure of slag. In particular, this paper focuses on low-rank coal and biomass that have been receiving increased attention recently. Besides, it reviews the available methodologies and formulae for slag viscosity measurement/prediction and summarizes the current limitations and potential applications. Moreover, it discusses the slagging behavior of different ranks of coal and biomass by examining the applicability of the current viscosity measurement methods to these fuels, and the viscosity prediction models and factors that affect the slag viscosity. This review shows that the existing viscosity models and slagging indices can only satisfactorily predict the viscosity and slagging propensity of high-rank coals but cannot predict the slagging propensity and slag viscosity of low-rank coal, and especially biomass ashes, even if they are limited to a particular composition only. Thus, there is a critical need for the development of an index, or a model or even a measurement method, which can predict/measure the slagging propensity and slag viscosity correctly for all low-rank coal and biomass ashes.

关键词： slag     viscosity     biomass     low-rank coal     combustion     gasification    

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Wheel tracking methods to evaluate moisture sensitivity of hot-mix asphalt mixtures

Jie HAN,Harihar Shiwakoti

《结构与土木工程前沿（英文）》 2016年 第10卷 第1期   页码 30-43 doi: 10.1007/s11709-016-0318-1

摘要： Existing test methods to determine moisture sensitivity in hot-mix asphalt (HMA) mixtures are time consuming and inconsistent. This research focused on wheel tracking devices to evaluate moisture sensitivity. The Asphalt Pavement Analyzer (APA) and the Hamburg Wheel Tracking Device (HWTD) were used for this research. Compacted cylindrical samples were fabricated using a Superpave Gyratory compactor. This study selected two most commonly used mixtures, SM-12.5A with PG 64-22 binder in overlay projects and SM-19A mixtures with PG 64-22 binder for major modification projects at Kansas Department of Transportation. Test results show that APA tests could induce stripping in most samples without any anti-stripping agent, which could be identified visually. However, APA results did not indicate any stripping inflection point while the HWTD results showed stripping inflection points, which are important to identify stripping potential of mixtures. The APA results show that wet tests are severe at lower temperatures. The HWTD results show improvement in the performance using anti-stripping agents at later stage. The HWTD test is more effective as a rapid test method in case of determining moisture sensitivity. Laboratory results from this study should be verified and correlated with field performance.

关键词： hot-mix asphalt     moisture sensitivity     rutting     wheel tracking test    

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标题 作者 时间 类型 操作

Effect of different high viscosity modifiers on rheological properties of high viscosity asphalt

期刊论文

新型高黏度改性沥青的研发和应用

杨林江

期刊论文

Linear viscoelastic behavior of asphalt binders and mixtures containing very high percentages of reclaimedasphalt pavement

期刊论文

Development and road performance of clear asphalt with high transparency and adhesion

期刊论文

saccharification and fermentation of sweet potato powder for the production of ethanol under conditions of very high

Yinxiu CAO, Hongchi TIAN, Kun YAO, Yingjin YUAN

期刊论文

Effect of carbon black on the dynamic moduli of asphalt mixtures and its master curves

Chuangmin LI, Fanbo NING, Yuanyuan LI

期刊论文

New approach to determine the plastic viscosity of self-compacting concrete

M. BENAICHA,X. ROGUIEZ,O. JALBAUD,Y. BURTSCHELL,A. Hafidi ALAOUI

期刊论文

Outdoor aging of road asphalt and SBS modified asphalt

Li XIANG, Juan TU, Jian CHENG, Guohe QUE

期刊论文

Fatigue of asphalt binder, mastic and mixture at low temperature

Dong WANG, Linbing WANG, Guoqing ZHOU

期刊论文

Effect of styrene-butadiene-styrene copolymer on the aging resistance of asphalt: An atomistic understanding

期刊论文

Hierarchical approach for fatigue cracking performance evaluation in asphalt pavements

Ibrahim ONIFADE, Yared DINEGDAE, Björn BIRGISSON

期刊论文

A dimensional analysis on asphalt binder fracture and fatigue cracking

Qian ZHAO, Zhoujing YE

期刊论文

The investigation of fly ash based asphalt binders using atomic force microscope

Rajan SAHA, Kyle MALLOY, Emil BAUTISTA, Konstantin SOBOLEV

期刊论文

A critical review of ash slagging mechanisms and viscosity measurement for low-rank coal and bio-slags

Md Tanvir ALAM, Baiqian DAI, Xiaojiang WU, Andrew HOADLEY, Lian ZHANG

期刊论文

Wheel tracking methods to evaluate moisture sensitivity of hot-mix asphalt mixtures

Jie HAN,Harihar Shiwakoti

期刊论文